The synthetic organic chemist's companion / (Record no. 40)
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| 000 -LEADER | |
|---|---|
| fixed length control field | 03779cam a2200205 a 4500 |
| 001 - CONTROL NUMBER | |
| control field | 853 |
| 005 - DATE AND TIME OF LATEST TRANSACTION | |
| control field | 20200611112637.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION | |
| fixed length control field | 070316s2007 njua b 001 0 eng |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER | |
| International Standard Book Number | 9780470107072 (cloth) |
| 040 ## - CATALOGING SOURCE | |
| Transcribing agency | DLC |
| 082 00 - DEWEY DECIMAL CLASSIFICATION NUMBER | |
| Classification number | 547.2 |
| Edition number | 22 |
| Item number | P672 |
| 100 1# - MAIN ENTRY--PERSONAL NAME | |
| Personal name | Pirrung, Michael C. |
| 245 14 - TITLE STATEMENT | |
| Title | The synthetic organic chemist's companion / |
| Statement of responsibility, etc | Michael C. Pirrung. |
| 260 ## - PUBLICATION, DISTRIBUTION, ETC. (IMPRINT) | |
| Place of publication, distribution, etc | Hoboken, N.J. : |
| Name of publisher, distributor, etc | Wiley-Interscience, |
| Date of publication, distribution, etc | 2007 |
| 300 ## - PHYSICAL DESCRIPTION | |
| Extent | xiii, 198 p. |
| Other physical details | ill. (some col.) ; |
| Dimensions | 23 cm. |
| 500 ## - GENERAL NOTE | |
| General note | Includes bibliographical references (p. 187-188) and index |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name as entry element | Organic compounds |
| General subdivision | Synthesis. |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) | |
| Koha item type | Books |
| 505 0# - FORMATTED CONTENTS NOTE | |
| Formatted contents note | Table of Contents<br/>Preface<br/>Acknowledgments<br/>Table of Contents<br/>1. Searching the Literature<br/>1.1. Commercial availability<br/>1.2. Literature preparations<br/>2. Reagents<br/> 2.1. Short path distillation<br/> 2.2. Ampules<br/> 2.3. Reagent solutions<br/> 2.4. Titration<br/> 2.5. Reagent storage<br/> 2.6. Subtle reagent variations<br/> 2.7. Dangerous reagents<br/> 2.8. Reagent properties<br/>3. Gases<br/> 3.1. Lecture bottles<br/> 3.2. Tanks or cylinders<br/> 3.3. Gas safety<br/>4. Reactions on a Small Scale ? 1-25 mmol<br/>4.1. Reaction flasks<br/>4.2. Stirring<br/>4.3. Glass joints<br/>4.4. Inert atmosphere<br/>4.5. Apparatus for addition<br/>4.6. Condensers<br/>4.7. Other equipment and considerations<br/>5. Temperature Control<br/>5.1. Heating<br/>5.2. Cooling<br/>6. Solvents<br/>6.1. Selection<br/>6.2. Purity<br/>6.3. Degassing<br/>6.4. Ammonia<br/>7. The Research Notebook<br/>8. Conducting the Reaction Itself<br/>8.1. Reagents supplied as dispersions<br/>8.2. Azeotropic drying<br/>8.3. Stoichiometry<br/>8.4. Syringe and inert atmosphere techniques<br/>8.5. General procedure for transfer of materials by syringe<br/>8.6. Addition<br/>8.7. Special techniques<br/> 8.7.1.Water removal<br/>8.7.2.Reactions above atmospheric pressure<br/>8.7.3.Reagent gases<br/>8.7.4.Ultrasonication<br/>8.8 Quenching <br/>8.9. Specialized reagents<br/>8.9.1. Diazomethane<br/>8.9.2. Lithium aluminum hydride<br/>8.9.3.Hydrogen peroxide<br/>8.10. Reaction time vs. purification time<br/>9. Following the Reaction<br/>9.1. Thin layer chromatography (TLC)<br/>9.1.1. Cutting glass TLC plates<br/>9.1.2. Spotting TLC plates<br/>9.1.3. Eluting TLC plates<br/>9.1.4. Visualizing TLC plates<br/>9.2. Gas chromatography (GC)<br/>9.3. High pressure liquid chromatography (HPLC)<br/>9.4. NMR spectroscopy<br/>10. Working Up Reactions<br/>10.1. Solvent extracation<br/>10.2. Drying organic solutions<br/>10.3. Specialized work-ups<br/>10.3.1. Reactions producing triphenylphosphine oxide<br/>10.3.2. Reactions involving boron compounds<br/>10.3.3. Reactions involving copper salts<br/>10.3.4. Reactions involving aluminum reagents<br/>10.3.5. Reactions involving tin reagents<br/>11. Evaporation<br/>12. Vacuum Systems<br/>12.1. Vacuum sources<br/>12.2. Vacuum manifolds<br/>12.3. Vacuum gauges<br/>13. Purification of Products<br/>13.1. Distillation<br/>13.2. Silica gel chromatography<br/>13.3. Flash column chromatography<br/>13.4. Gradients<br/>13.5. Special absorbents<br/>13.5.1. Triethylamine-treated silica gel<br/>13.5.2. Oxalic acid-coated silica gel<br/>13.5.3. Silver nitrate-impregnated silica gel<br/>13.5.4. Other sorbents<br/>13.6. Preparative gas chromatography<br/>14. Methods for Structure Elucidation<br/>14.1. Nuclear magnetic resonance spectroscopy<br/>14.2. Infrared spectroscopy (IR)<br/>14.3. Ultravilolet spectroscopy (UV)<br/>14.4. Combustion analysis<br/>14.5. Mass spectrometry<br/>14.6. Crystallography<br/>15. Cleaning Up After the Reaction<br/>16. Specific Examples<br/>16.1. The experimental<br/>16.2. The Org. Syn. Prep<br/>16.3. Comparison<br/>17. Strategies for Reaction Organization<br/>Appendices<br/>1. NMR spectral data of common contaminants of organic reaction products<br/>2. Synthetic solvent selection chart<br/>3. Recipes for TLC stains<br/>4. Mixotropic series<br/>5. Stuck joints<br/>6. Acidities of organic functional groups<br/>7. Acidities of organic functional groups in DMSO<br/>8. Web resources for synthetic chemistry<br/> |
| Withdrawn status | Damaged status | Not for loan | Home library | Current library | Date acquired | Source of acquisition | Full call number | Barcode | Date last seen | Price effective from | Koha item type |
|---|---|---|---|---|---|---|---|---|---|---|---|
| UE-Central Library | UE-Central Library | 17.05.2018 | U.E. | 547.2 P672 | T853 | 17.05.2018 | 17.05.2018 | Books |
