Includes bibliographical references and index.

1. Part 1 Fundamentals: Data Collection and Analys
2. Chapter 1 Working with Experimental Data
3. Collecting the Data, 1
4. Keeping a Notebook, 1
5. 'Cornputer Files, 2
6. On-the-Fly Estimation, 2
7. Data Treatment, 2
8. Elementary Statistical Concepts,
9. Dieterining lhndivid al Standaif rd Uncert,il ties 9
10. Combining Standard Uncertainties: Propagation of Error, 18
11. Least Squares and Parameter Estimation, 26
12. Physical Models: General Definitions and Examples, 26
13. Desiderata, 28
14. Basis of Least Squares Approach, 28
15. Data Values and Unzcrtainties: Unk nown, K notu n, and
16. Relative Errors, 29
17. Li iear and Nonlinear Models, 31
18. Requirements on Fitting Program s, 31
19. How the Fit Works, 32
20. Checking the Fit, 33
21. Example: Flourescence Lifetime, 34
22. Using the Output: Uncertainties and Covariances
23. In the tfitped Pirart iters, 36
24. Pathology, 36
25. Using and Presenting the Results, 37
26. Comparison Tests, 37
27. Expanded Uncertainties and C onfidence L eves, 9
28. Systematic and Related Errors, 41
29. Reporting Your Work, 45
30. Chapter 2 Data Analysis in the Physical Chemistry Laboratory:
31. The Use of a Scientific Spreadsheet
32. Data Analysis by Computer, 51
33. Data Entry and Transformnation, 5
34. Graphing the Data., 53
35. Regression Analysis of the Data, 54
36. ( her SIDA Features, .
37. Numerical Analysis: Use of the Excel Solver, 63
38. Chapter 3 7itemperature. Pressure, Voltgr c Aicasiurcmenties, av il
39. Dctetction
40. Temperature, 67
41. A4erc ury-il-( clatss Ther i ot u /n'o )
42. 'Theur7)oco tpe, 69
43. Resistance Therinoine1te;s, -1
44. R sistl7j:C +T CO 7Jl() l77 i0[ ,:;-[
45. Semitkonductoer Teip C/ratiure ras2 us ',0
46. Noncontact 7-emp/erature Mleasur'.mq ; 7c 2
47. Pressure, 73
48. Definitflon and runits, 73
49. Pressuil ' maleasuinl2 Device?S, 73
50. Voltage Measurements, 78
51. Coinp'ter-r ssistci Data Acql's itfon 79
52. Pinary Nu, hibrs, 1S /
53. Light Detectioni 82
54. Photodiide, 82
55. Part 2 Thermodynamics of Gases
56. Experimnrent I Thermodynaics o- a Gas Phase Reacti,on: Re,versti
57. Dissociation of N )Ot
58. Experiment 2 ,ati Capacity Ratio ( C,/Cv) of Gses
59. Experiment 3 Real Gases, Part I 1e )he j e-Tihorison Coeff ici.
60. Experiment 4 Re'al Gases, Part I: ihe Second \Vinria Co l-icjcicm
61. Part 3 Thermochemistry
62. Experiment 5 Bomb Calorietry: Heat of Fr-orattion of 4 \m tl'lalcn,
63. Or Sucrose
64. Experimtent 6 Bomb Calorim etry: D)cterminaton of thc Resonan.ce Ynerrgl
65. Of Beinzene
66. Part 4 Thermodynamics of Solutions. Eect rochem stry
67. Expermle nt 7 1c fitr y (Af M\ixing
68. "Expri " ent 8 l Therod ynamis of an Electrochi ia  coil P' r - , 1 .
69. Fl'nthlal y, and E i tropy of Reactit i
70. Expcriment 9 Therniodynammics oof an Electrocherncal c'el, Par
71. Uandard Cel Potential and Activity (Co rh cl'
72. Part 5 Thermodynamics of Phase Equilibrium and :olutio Prnot
73. Exreri ment .10 Mutm u Solu bilties of liqunjai K at
74. Expcriment I1 he Vapor Pressure and C<.r hit Of
75. Expenient 1.2 liquicviapor Cof I i o S
76. Critical Point
77. Experiment 13 Solid-Liquid Equilibrium in a Binary System
78. Experiment 14 Liquid-Vapor Equilibrium in a Binary System
79. Experiment 15 Henry's Law Constant Determined by Headspace
80. Chromatography
81. Experiment 16 Surface Tension Properties of Liquids
82. Part 6 Transport Properties and Chemical Kinetics
83. Experiment 17 Viscosity of Liquids, Part 1: Low Viscosities
84. Experiment 18: Viscosity of Liquids, Part II: High Viscosities
85. Experiment 19: Determination or Collision Diameters from Gas Viscosities
86. Experiment 20: Kinetics of a Homogeneous Reaction in i Sotion
87. Experiment 21: Kinetics of a Diffusion-Controlled Reaction
88. Experiment 22: Kinetics of a Reversible, First-Order, Consecutive
89. Reaction: The Reduction of Cr(V) by cglutathione
90. Experiment 23: Kinetics of an Enzyme-Catalyzed Reaction
91. Experiment 24: Kinetics and Thermodynamics of a Heterogeneous Gas
92. Phase Reaction: Reversible Dissociation of Ammonium
93. Carbamate
94. Experiment 25: Kinetics and Mechanism of a Heterogenous Reaction: Oxidation
95. Of Magnesium by Hydrochloric Acid
96. Experiment 26: Laser Kinetics, Part 1: Luminescence Quenching of the
97. Uranyl Ion by the Chloride Ion
98. Experiment 27: Laser Kinetics, Part I: Photochromism of Mercury(IH)
99. Dithizonate
100. Experiment 28: Laser Kinetics, Part Ill: Viscosity Effects on Luminescence
101. Quenching Rate Constants
102. Part 7 Colloidal Systems: Micelles
103. Experiment 29: Determination of the Critical Micelle Concentration
104. Experiment 30: Determination of the Mean Aggregation Number of a
105. Micellar System
106. Part 8 Pol mers
107. Experiment 31: Molecular Weight and Monomer Linkage Properties of
108. Poly(vinyl alcohol)
109. Experiment 32: Thermodynamic Properties of Elastomers
110. Part .9 .Photophysics and Molecuar Spectroscopy
111. Experiment 33: Excited-State Properties of 2-Naphthol, Part 1: excited-State
112. Acidity Constant
113. Experimnent 34: F ltd &state P roper s P atr f: De tp-ton"ro
114. And Protornation Rate n tat
115. Experiment 35: Enthalpy and Entropv of Extncr Iom
116. Experiment 36: Rotat o n-viibrational Sectru.i of P
117. Experiment 37: 'ibrarional Spectrun oat Snfr: )i,
118. Experiment 38: analysis of a lnme us Eisn S o
119. Experiment 39: Absorption Spctr nr (oaf Co-4
120. Part 10 Computational Chemistry
121. Experinent 40: Computational Ch( cistry Calcuri' of A A, G r,
122. And AIS0 for the Rcaki:on u N:O , :2 ? J
123. Experiment 41: (comnputatinal Detcmu tn o 'Co
124. Of HCI